GC-DFPD双火焰光度检测器DFPD分析纯苯中痕量噻吩,芝麻香白酒,3-甲硫基丙醇,室内空气,焦炉煤气,炼厂气,天然气,变压器油,多氯联苯,植物油,6号溶剂残留,热解吸仪,氨水
GC-DFPD
双火焰光度检测器DFPD分析纯苯中痕量噻吩
火焰光度检测器(FPD)是一种高灵敏度高选择性的测定硫磷化物的气相色谱检测器。但是FPD测硫时的选择性并不好,在测低浓度硫化物时灵敏度也不高,且线性较差。因此,当试样中含有大量烃类时,必须用色谱柱把烃类与硫化物完全分离,此时的选择性(S/C)为10~4,否则就会受到烃类的严重干扰,甚信号完全消失。
滕州市浩瀚色谱仪器技术服务有限公司,,以科学发展为指导,,,色谱工程研究所,分析与测试中心,3个科研单位,研制成功GC-DFPD双火焰光度检测器DFPD分析纯苯中痕量噻吩 。该检测器具有上、下两个火焰,下火焰为一富氧焰,用于将有机硫、磷化合物及烃类氧化生成相应的氧化物;上火焰为一富氢空气焰,可将有机硫、磷氧化物还原为S2、HPO等化学发光分子。而烃类的氧化产物,如CO2、H2O等无光信号,所以DFPD能够排除烃类干扰,而选择性地测量硫磷化合物。在作定量分析时,硫信号严格与硫化物浓度的平方成线性关系(或信号的平方根与浓度成线形关系),对硫的响应值是10-12克/秒,对硫的响应值是10-11克/秒。同时该检测器具有双光路系统,实现一次进样同步检测含硫和磷化合物。因此DFPD具有灵敏度高、选择性好、响应时间快、分析效率高、可以接毛细管柱、填充柱等特点,所以在环境保护、工程科学、食品中的检验,以及农残留量检验等方面得到了广泛的应用。
浩瀚色谱,同时供应:火焰光度检测器FPD
氢火焰检测器FID
热导检测器TCD
电子捕获检测器ECD
氮磷检测器NPD
GC-DFPD双火焰光度检测器DFPD分析纯苯中痕量噻吩:
纯苯中痕量噻吩测定谱图:
Analysis of Trace Thiophene in Benzene by GC-DFPD Dual Flame Photometric Detector
Flame Photometric Detector (FPD) is a high sensitivity and high selectivity gas chromatographic detector for the determination of sulfur phosphide. However, the selectivity of FPD is not good, the sensitivity is not high when the concentration of sulfide is measured, and the linearity is poor. Therefore, when the sample contains a large number of hydrocarbons, you must use the column to completely separate the hydrocarbons and sulfides, the selectivity (S / C) of 10 to 4, otherwise it will be severely interfered by hydrocarbons, Even the signal completely disappeared.
Tengzhou City, the vast chromatography Instrument Technology Service Co., Ltd., advancing with the times, under the guidance of scientific development, under the leadership of Wang Xiaoying manager, relying on Xiangying Analytical Technology Research Institute, Chromatography Engineering Research Center, Analysis and Testing Center, 3 scientific research units , The successful development of GC-DFPD dual flame photometric detector for the analysis of trace benzene in thiophene. The new detector has two upper and lower flames, the lower flame is an oxygen-enriched flame, used for organic sulfur, phosphorus compounds and hydrocarbons to generate the corresponding oxide; the flame is a hydrogen-rich air flame, organic Sulfur, phosphorus oxide reduced to S2, HPO and other chemiluminescent molecules. While the oxidation products of hydrocarbons such as CO2, H2O and other non-optical signals, so DFPD can exclude hydrocarbon interference, and selective measurement of sulfur phosphorus compounds. For quantitative analysis, the sulfur signal is linearly proportional to the square of the sulfide concentration (or the square root of the signal is linearly related to the concentration), the response to sulfur is 10-12 g / s, the response to sulfur is 10 -11 g / sec. At the same time the detector has a dual-beam system, to achieve a simultaneous injection of sulfur and phosphorus compounds. So DFPD has high sensitivity, good selectivity, fast response time, high efficiency, can be connected to the capillary column, packed column and so on, so in environmental protection, engineering science, food testing, and pesticide residue test A wide range of applications.
The vast spectrum, while supply: flame photometric detector FPD
Hydrogen Flame Detector
Thermal conductivity detector
Electron Capture Detector
NPD Detector
GC-DFPD Dual Flame Photometric Detector for Analysis of Trace Thiophene in Benzene:
Determination of trace thiophene in pure benzene: