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4mm*0.8m药典二氧化碳 玻璃球为填料的色谱柱(0.8m×4mm,80目)

4mm*0.8m药典二氧化碳 玻璃球为填料的色谱柱(0.8m×4mm,80目)

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产品名称:4mm*0.8m药典二氧化碳 玻璃球为填料的色谱柱(0.8m×4mm,80目)

产品型号:4mm*0.8m药典二氧化碳

产品厂商:浩瀚色谱(山东)应用技术开发有限公司

简单介绍

玻璃球为填料的色谱柱(0.8m×4mm,80目),液化石油气,二甲醚,甲缩醛,乙缩醛,乙醇,室内空气,焦炉煤气,炼厂气,天然气,变压器油,多氯联苯,植物油,增塑剂,塑化剂,消毒剂

4mm*0.8m药典二氧化碳 玻璃球为填料的色谱柱(0.8m×4mm,80目)的详细介绍

玻璃球为填料的色谱柱(0.8m×4mm,80目)
玻璃球为填料的色谱柱(0.8m×4mm,80目) 详细信息:


碳氢化合物 取本品作为供试品;取甲烷含量为0.0020%的气体(以氮气为稀释剂)作为对照气体,照气相色谱法(通则0521)试验,用玻璃球为填料的色谱柱(0.8m×4mm,80目);柱温为110℃;进样口温度为110℃;检测器温度为120℃。量取供试品气体与对照气体,注入气相色谱仪,在净化温度为360℃时测得的峰面积为相应空白值;量取供试品气体与对照气体,注入气相色谱仪,测定峰面积,减去相应空白值后的峰面积为校正峰面积。按外标法以校正峰面积计算,含碳氢化合物(以甲烷计)不得过0.0020%。

名称:玻璃球填充柱

规格:0.8m*4mm,80目

型号:HH-BLQ

高使用温度:320°C

浩瀚色谱(山东)应用技术开发有限公司以医用二氧化碳中碳氢化合物杂质为例,使用欧洲药典中提供的两种不同的检测方法对杂质进行测定。对比结果表明,色谱、光谱等仪器类方法的杂质检出限更低,重复性和中间精密度也更好。气体检测管系统操作简单、用气量少,适用于对检测限等要求不高的检测需求。仪器法和检测管法都是实用的医用二氧化碳中杂质的检测手段,可根据需求选用不同的方法实施检测。

玻璃球为填料的色谱柱(0.8m×4mm,80目) 测试谱图:



Pharmacopoeia Determination of hydrocarbons in carbon dioxide Glass ball chromatographic column

Pharmacopoeia Carbon Dioxide Determination Glass Ball Chromatographic Column Details:



Name: glass ball filled column



Specification: 0.8m * 4mm, 80 meshes



Model: HH-BLQ



Maximum operating temperature: 320 ° C



Taking hydrocarbon impurities in medical carbon dioxide as an example, Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. uses two different detection methods provided in European Pharmacopoeia to determine impurities. The comparison results show that the impurity detection limits of chromatographic, spectroscopic and other instrumental methods are lower, and the repeatability and intermediate precision are better. The gas detection tube system is simple to operate, with less gas consumption, and is suitable for detection needs that do not require high detection limits. Instrument method and detection tube method are both practical detection methods for impurities in medical carbon dioxide, and different methods can be selected for detection according to needs.



Pharmacopoeia Determination of Hydrocarbons in Carbon Dioxide Glass Ball Chromatographic Column Test Spectrum:

Chromatographic column packed with glass ball (0.8m × 4mm, 80 meshes)

Chromatographic column packed with glass ball (0.8m × 4mm, 80 meshes) Details:



Hydrocarbon Take this product as the test sample; Take the gas with 0.0020% methane content (nitrogen as diluent) as the reference gas, test according to the gas chromatography method (General Rule 0521), and use the glass ball as the packing column (0.8m × 4mm, 80 meshes); The column temperature is 110 ℃; The injection port temperature is 110 ℃; The detector temperature is 120 ℃. Measure the test gas and reference gas, inject them into the gas chromatograph, and the peak area measured at the purification temperature of 360 ℃ is the corresponding blank value; Measure the test sample gas and the reference gas, inject them into the gas chromatograph, and measure the peak area. The peak area after subtracting the corresponding blank value is the corrected peak area. The hydrocarbon content (calculated by methane) shall not exceed 0.0020% according to the corrected peak area calculated by external standard method.


Name: glass ball filled column


Specification: 0.8m * 4mm, 80 meshes


Model: HH-BLQ


Maximum operating temperature: 320 ° C


Taking hydrocarbon impurities in medical carbon dioxide as an example, Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. uses two different detection methods provided in European Pharmacopoeia to determine impurities. The comparison results show that the impurity detection limits of chromatographic, spectroscopic and other instrumental methods are lower, and the repeatability and intermediate precision are better. The gas detection tube system is simple to operate, with less gas consumption, and is suitable for detection needs that do not require high detection limits. Instrument method and detection tube method are both practical detection methods for impurities in medical carbon dioxide, and different methods can be selected for detection according to needs.


Chromatographic column packed with glass ball (0.8m × 4mm, 80 mesh) test spectrum:

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